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C23H23N2O2(1+)*Br(1-)

Base Information Edit
  • Chemical Name:C23H23N2O2(1+)*Br(1-)
  • CAS No.:1412271-07-8
  • Molecular Formula:Br*C23H23N2O2
  • Molecular Weight:439.352
  • Hs Code.:
  • Mol file:1412271-07-8.mol
C<sub>23</sub>H<sub>23</sub>N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>*Br<sup>(1-)</sup>

Synonyms:C23H23N2O2(1+)*Br(1-)

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Chemical Property of C23H23N2O2(1+)*Br(1-) Edit
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Technology Process of C23H23N2O2(1+)*Br(1-)

There total 9 articles about C23H23N2O2(1+)*Br(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1: thionyl chloride / 0.67 h / 80 °C
2: aluminum (III) chloride / 1,2-dichloro-ethane / 0.5 h / 20 °C / Cooling with ice
3: sodium tetrahydroborate / ethanol; dichloromethane / 4 h / 0 - 20 °C
4: thionyl chloride / dichloromethane / 2 h / 0 - 20 °C
5: 1,4-dioxane / Reflux
6: toluene / Reflux
With aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; In 1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.2174/1570180811310070003
Guidance literature:
Multi-step reaction with 8 steps
1: piperidine / pyridine / 4 h / Reflux
2: palladium 10% on activated carbon; hydrogen / acetic acid / 1 h / 20 °C
3: thionyl chloride / 0.67 h / 80 °C
4: aluminum (III) chloride / 1,2-dichloro-ethane / 0.5 h / 20 °C / Cooling with ice
5: sodium tetrahydroborate / ethanol; dichloromethane / 4 h / 0 - 20 °C
6: thionyl chloride / dichloromethane / 2 h / 0 - 20 °C
7: 1,4-dioxane / Reflux
8: toluene / Reflux
With piperidine; aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; palladium 10% on activated carbon; hydrogen; In 1,4-dioxane; pyridine; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; toluene;
DOI:10.2174/1570180811310070003
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