C₂₁H₃₆N₂O₂SeSi

Base Information

• Chemical Name: C₂₁H₃₆N₂O₂SeSi
• CAS No.: 1044259-87-1
• Molecular Formula: C₂₁H₃₆N₂O₂SeSi
• Molecular Weight: 455.575
• Mol file: 1044259-87-1.mol

Synonyms:C₂₁H₃₆N₂O₂SeSi

Chemical Property of C₂₁H₃₆N₂O₂SeSi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂₁H₃₆N₂O₂SeSi

There total 1 articles about C₂₁H₃₆N₂O₂SeSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

cyclohexyl isoselenocyanate (4426-69-1) + (3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one (85254-20-2) → C21H36N2O2SeSi (1044259-87-1)

Guidance literature:

(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one; With sodium hydride; In tetrahydrofuran; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere;

cyclohexyl isoselenocyanate; In tetrahydrofuran; mineral oil; at -10 ℃; Inert atmosphere;

DOI:10.1021/ol801010y

Reference yield: 84.0%

C21H36N2O2SeSi (1044259-87-1) → C21H35IN2O2SeSi (1254833-42-5)

Guidance literature:

With iodine; In dichloromethane; at 20 ℃; for 11.5h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol801010y

upstream raw materials:

cyclohexyl isoselenocyanate

(3S,4R)-3-{(1R)-{[tert-butyl(dimethyl)silyl]oxo}ethyl-4-prop-2-yn-1-yl}azetidine-2-one

Downstream raw materials:

C₂₁H₃₅IN₂O₂SeSi