Technology Process of C24H31NO4S
There total 13 articles about C24H31NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H29NO4S;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
methyl iodide;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 15h;
DOI:10.1021/ol300571b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium phosphate; copper(ll) sulfate pentahydrate; 1,10-Phenanthroline / toluene / 44 h / 60 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
3.2: 15 h / -78 - 20 °C
With
potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol300571b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 0.5 h / 185 °C / Neat (no solvent)
2.1: potassium phosphate; copper(ll) sulfate pentahydrate; 1,10-Phenanthroline / toluene / 44 h / 60 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C
4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
4.2: 15 h / -78 - 20 °C
With
potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol300571b
