isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate

Base Information

Chemical Name:isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate
CAS No.:321691-00-3
Molecular Formula:C₁₅H₁₈N₂O₂S
Molecular Weight:290.386
Hs Code.:
Mol file:321691-00-3.mol

Synonyms:5-isoisopropoxycarbonyl-6-methyl-4-phenyl-3,4-dihydropyrimidihydropyrimidin-2(1H)-thione

Suppliers and Price of isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate

There total 1 articles about isopropyl 6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydro-5-pyrimidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 542-08-5
isopropyl acetoacetate

: 100-52-7
benzaldehyde

: 17356-08-0
thiourea

: 321691-00-3
5-isoisopropoxycarbonyl-6-methyl-4-phenyl-3,4-dihydropyrimidihydropyrimidin-2(1H)-thione

Guidance literature:: With calcium fluoride; In ethanol; at 40 ℃; for 2h;
DOI:10.1016/j.tetlet.2009.02.162

Reference yield: 89.0%

: 321691-00-3
5-isoisopropoxycarbonyl-6-methyl-4-phenyl-3,4-dihydropyrimidihydropyrimidin-2(1H)-thione

: 108-95-2,27073-41-2
phenol

: isopropyl 4-methyl-2-phenoxy-6-phenylpyrimidine-5-carboxylate

Guidance literature:: With copper diacetate; silver carbonate; In toluene; at 80 ℃;
DOI:10.1039/d1ra07713a

Reference yield: 86.0%

: 321691-00-3
5-isoisopropoxycarbonyl-6-methyl-4-phenyl-3,4-dihydropyrimidihydropyrimidin-2(1H)-thione

: 62-53-3
aniline

: isopropyl 6-methyl-4-phenyl-2-phenylaminopyrimidine-5-carboxylate

Guidance literature:: With copper(I) thiophene-2-carboxylate; palladium diacetate; lithium hexamethyldisilazane; In toluene; at 100 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02617