phenyl 2-(trimethylsilyl)ethyl phthalate

Base Information

• Chemical Name: phenyl 2-(trimethylsilyl)ethyl phthalate
• CAS No.: 1416009-54-5
• Molecular Formula: C₁₉H₂₂O₄Si
• Molecular Weight: 342.467
• Mol file: 1416009-54-5.mol

Synonyms:phenyl 2-(trimethylsilyl)ethyl phthalate

Chemical Property of phenyl 2-(trimethylsilyl)ethyl phthalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of phenyl 2-(trimethylsilyl)ethyl phthalate

There total 1 articles about phenyl 2-(trimethylsilyl)ethyl phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) → phenyl 2-(trimethylsilyl)ethyl phthalate (1416009-54-5)

Guidance literature:

Multi-step reaction with 2 steps

2: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1021/jo301698v

Reference yield:

phenyl 2-(trimethylsilyl)ethyl phthalate (1416009-54-5) → benzene-1,2-dicarboxylic acid (88-99-3,73607-73-5) + phenol (108-95-2,27073-41-2)

Guidance literature:

phenyl 2-(trimethylsilyl)ethyl phthalate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; dimethylsulfoxide-d6; for 4h;

With water-d2; In tetrahydrofuran; dimethylsulfoxide-d6;

DOI:10.1021/jo301698v

upstream raw materials:

phthalic anhydride

Downstream raw materials:

benzene-1,2-dicarboxylic acid

phenol