2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

Base Information

• Chemical Name: 2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide
• CAS No.: 1293997-75-7
• Molecular Formula: C₁₈H₂₁N₃O₂
• Molecular Weight: 311.384

Synonyms:2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

Chemical Property of 2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

Chemical Property:

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Technology Process of 2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

There total 1 articles about 2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-cyano-3-phenylacrylamide (709-79-5) + dimedone (126-81-8) → 2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide (1293997-75-7)

Guidance literature:

With ammonium acetate; acetic acid; for 5h; Reflux;

DOI:10.3184/030823410X12852490447544

Reference yield: 75.0%

2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide (1293997-75-7) + acetic anhydride (108-24-7) → 2,8,8-trimethyl-5-phenyl-7,8,9,10-tetrahydropyrimido[4,5-b]quinoline-4,6(3H,5H)-dione (1232790-09-8)

Guidance literature:

With pyridine; for 3h; Reflux;

DOI:10.3184/030823410X12852490447544

Reference yield: 75.0%

2-amino-7,7-dimethyl-5-oxo-4-phenyl-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide (1293997-75-7) + phenyl isothiocyanate (103-72-0) → 8,8-dimethyl-3,5-diphenyl-2-thioxo-2,3,7,8,9,10-hexahydropyrimido[4,5-b]quinoline-4,6(1H,5H)-dione (1293997-85-9)

Guidance literature:

With acetic acid; for 4h; Reflux;

DOI:10.3184/030823410X12852490447544

upstream raw materials:

2-cyano-3-phenylacrylamide

dimedone

Downstream raw materials:

8,8-dimethyl-5-phenyl-7,8,9,10-tetrahydro[1,2,3]triazino[4,5-b]quinoline-4,6(3H,5H)-dione

8',8'-dimethyl-5'-phenyl-7',8',9',10'-tetrahydro-1'H-spiro[cyclohexane-1,2'-pyrimido[4,5-b]quinoline]-4',6'(3'H,5'H)-dione

2,8,8-trimethyl-5-phenyl-7,8,9,10-tetrahydropyrimido[4,5-b]quinoline-4,6(3H,5H)-dione

8,8-dimethyl-3,5-diphenyl-2-thioxo-2,3,7,8,9,10-hexahydropyrimido[4,5-b]quinoline-4,6(1H,5H)-dione

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