2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

Base Information

Chemical Name:2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride
CAS No.:1246852-77-6
Molecular Formula:C₁₆H₂₀BrNO*ClH
Molecular Weight:358.706
Hs Code.:

Synonyms:2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

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Chemical Property of 2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

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Technology Process of 2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

There total 6 articles about 2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1246852-76-5
1-(4-(4-bromophenyl)bicyclo[2.2.2]octan1-yl)-2-chloroethanone

: 1246852-77-6
2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

Guidance literature:: 1-(4-(4-bromophenyl)bicyclo[2.2.2]octan1-yl)-2-chloroethanone; With sodium diformamide; potassium iodide; In tetrahydrofuran; at 20 ℃; for 20h;

With hydrogenchloride; In methanol; water;

Reference yield:

: 18720-35-9
bicyclo[2.2.2]octane-1,4-dicarboxylic acid monomethyl ester

: 1246852-77-6
2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / dichloromethane / 3.5 h / Reflux

2: aluminum (III) chloride / 16 h / 20 °C / Reflux

3: bromine; silver trifluoroacetate / chloroform / 2 h / 20 °C

4: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C

5: potassium iodide; sodium diformamide / tetrahydrofuran / 20 h / 20 °C

With aluminum (III) chloride; sodium diformamide; bromine; silver trifluoroacetate; potassium iodide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; chloroform;

Reference yield:

: 23062-51-3
methyl 4-bromo-bicyclo[2.2.2]octane-1-carboxylate

: 1246852-77-6
2-amino-1-(4-(4-bromophenyl)bicyclo[2.2.2]octan-1-yl)ethanone hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / 16 h / 20 °C / Reflux

2: bromine; silver trifluoroacetate / chloroform / 2 h / 20 °C

3: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C

4: potassium iodide; sodium diformamide / tetrahydrofuran / 20 h / 20 °C

With aluminum (III) chloride; sodium diformamide; bromine; silver trifluoroacetate; potassium iodide; lithium diisopropyl amide; In tetrahydrofuran; chloroform;