cinnamylidene ethyl cyanoacetate

Base Information

Chemical Name:cinnamylidene ethyl cyanoacetate
CAS No.:32302-69-5
Molecular Formula:C₁₄H₁₃NO₂
Molecular Weight:227.263
Hs Code.:

Synonyms:cinnamylidene ethyl cyanoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cinnamylidene ethyl cyanoacetate

Chemical Property:

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Technology Process of cinnamylidene ethyl cyanoacetate

There total 3 articles about cinnamylidene ethyl cyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 14371-10-9
(E)-3-phenylpropenal

: 105-56-6
ethyl 2-cyanoacetate

: 32302-69-5
cinnamylidene ethyl cyanoacetate

Guidance literature:: With sodium nitrate; fluorapatite; at 20 ℃; for 0.416667h;
DOI:10.1081/SCC-100103527

Reference yield: 80.0%

: 104-55-2
3-phenyl-propenal

: 105-56-6
ethyl 2-cyanoacetate

: 32302-69-5
cinnamylidene ethyl cyanoacetate

Guidance literature:: aluminum oxide; In ethanol; for 0.666667h; Heating;
DOI:10.1081/SCC-120016322

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 32302-69-5
cinnamylidene ethyl cyanoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen / toluene / 2 h / 59.84 °C / 750.08 Torr

2: Ru/layered double hydroxide growth on graphene oxide nanocomposite / toluene / 3 h / 59.84 °C

With oxygen; In toluene; 2: |Knoevenagel Condensation;
DOI:10.1002/cctc.201901208