2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

Base Information

Chemical Name:2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate
CAS No.:1097936-08-7
Molecular Formula:C₄H₁₁N*C₁₁H₁₃ClFO₆P
Molecular Weight:399.784
Hs Code.:

Synonyms:2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

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Chemical Property of 2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

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Technology Process of 2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

There total 3 articles about 2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: O,O-dimethyl 1-(2-chloro-4-fluorophenoxyacetoxy)ethylphosphonate

: 75-64-9
tert-butylamine

: 1097936-08-7
2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

Guidance literature:: at 20 ℃;
DOI:10.1080/10426507.2012.736101

Reference yield:

: 826990-46-9
2-(2-chloro-4-fluorophenoxy)acetyl chloride

: 1097936-08-7
2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: 20 °C

With pyridine; In dichloromethane;
DOI:10.1080/10426507.2012.736101

Reference yield:

: 399-41-7
2-(2-chloro-4-fluorophenoxy)acetic acid

: 1097936-08-7
2-methylpropan-2-aminium methyl (1-(2-(2-chloro-4-fluorophenoxy)acetoxy)ethyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride

2: pyridine / dichloromethane / 0 - 20 °C

3: 20 °C

With pyridine; thionyl chloride; In dichloromethane;
DOI:10.1080/10426507.2012.736101