10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:1338685-20-3
Molecular Formula:C₂₈H₂₆N₄O₃
Molecular Weight:466.539
Hs Code.:

Synonyms:10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

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Chemical Property of 10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Chemical Property:

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Technology Process of 10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 7 articles about 10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61066-33-9,61066-34-0,61066-35-1,61127-23-9
pyrimidine-2,4,5,6(1H,3H)-tetraone

: 1338685-24-7
N-[2-(benzyloxy)-3-phenylpropyl]-4,5-dimethylbenzene-1,2-diamine

: 1338685-20-3
10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: With boric acid; acetic acid; at 20 ℃; for 18h;

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 1338685-20-3
10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide / water / 0.5 h / 70 °C

1.2: 0.25 h / -5 °C

1.3: 0 - 70 °C

2.1: caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

3.1: zinc; ammonium chloride / methanol / 0.08 h / 0 °C

4.1: boric acid; acetic acid / 18 h / 20 °C

With hydrogen bromide; boric acid; ammonium chloride; caesium carbonate; acetic acid; bis[2-(diphenylphosphino)phenyl] ether; zinc; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In methanol; water; toluene;

Reference yield:

: 4436-24-2
1,2-epoxy-3-phenylpropane

: 1338685-20-3
10-[2-(benzyloxy)-3-phenylpropyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide; water / N,N-dimethyl-formamide / 18 h / 65 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: trimethylphosphane / tetrahydrofuran / 18.5 h / 0 - 20 °C

3.2: 20 °C

4.1: caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

5.1: zinc; ammonium chloride / methanol / 0.08 h / 0 °C

6.1: boric acid; acetic acid / 18 h / 20 °C

With sodium azide; water; boric acid; sodium hydride; ammonium chloride; caesium carbonate; acetic acid; bis[2-(diphenylphosphino)phenyl] ether; zinc; trimethylphosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; mineral oil;