N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

Base Information

Chemical Name:N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester
CAS No.:93218-76-9
Molecular Formula:C₄₀H₄₈N₄O₁₁
Molecular Weight:760.841
Hs Code.:

Synonyms:N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

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Technology Process of N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

There total 7 articles about N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 62853-36-5,71822-09-8,85546-24-3
L-alanyl-(γ-benzyl ester D-isoglutamine)

: 74842-55-0
N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramic acid

: 93218-76-9
N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1016/0008-6215(84)85224-6

Reference yield:

: 18800-73-2,19238-66-5
benzyl (R)-5-amino-4-((tert-butoxycarbonyl)amino)-5-oxopentanoate

: 93218-76-9
N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid, p-toluenesulfonic acid / 0.33 h

2: triethylamine / various solvent(s) / 1.) 24 h, 0 deg C, 2.) room temperature, 24 h

3: trifluoroacetic acid, , p-toluenesulfonic acid / 0.33 h

4: 80 percent / triethylamine, benzotriazol-1-ol, dicyclohexylcarbodiimide / dimethylformamide; various solvent(s) / 24 h / Ambient temperature

With benzotriazol-1-ol; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85224-6

Reference yield:

: 18814-49-8
tert-butoxycarbonyl-L-alanyl-D-isoglutamine benzyl ester

: 93218-76-9
N-acetyl-1-O-benzyl-4,6-O-benzylidenemuramoyl-L-alanyl-D-idoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid, , p-toluenesulfonic acid / 0.33 h

2: 80 percent / triethylamine, benzotriazol-1-ol, dicyclohexylcarbodiimide / dimethylformamide; various solvent(s) / 24 h / Ambient temperature

With benzotriazol-1-ol; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85224-6