1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

Base Information

Chemical Name:1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole
CAS No.:1296274-53-7
Molecular Formula:C₃₂H₃₄N₂P₂
Molecular Weight:508.583
Hs Code.:

Synonyms:1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

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Chemical Property of 1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

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Technology Process of 1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

There total 1 articles about 1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1296274-52-6
ClP(N(C₆H₃(CH₃)2)CCH₃)2

: 829-85-6
diphenylphosphane

: 1296274-53-7
1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

Guidance literature:: diphenylphosphane; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

ClP(N(C₆H₃(CH₃)2)CCH₃)2; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/om200069t

Reference yield: 38.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 1296274-53-7
1,3-bis(2,6-dimethylphenyl)-4,5-dimethyl-2-(diphenylphosphino)-2,3-dihydro-1,3,2-diazaphosphole

: 107-13-1,25014-41-9
acrylonitrile

: 1296274-55-9
[Cl₂Pd(2-[1,3-bis(2',6'-dimethylphenyl)[1.3.2]diazaphospholenyl]-3-(diphenylphosphino)propanenitrile)]

Guidance literature:: In tetrahydrofuran; dichloromethane; (Ar); addn. of acrylonitrile to stirred soln. of 1,3-bis(2',6'-dimethylphenyl)-4,5-dimethyl-2-diphenylphosphino(1.3.2)diazaphospholene in THF, stirring at 50°C for 4 h, slow addn. of soln. (cod)PdCl2 in CH2Cl2, stirring for 0.5 h; evapn. under reduced pressure, extn. with Et2O, filtration, evapn. of solvent; elem. anal.;
DOI:10.1021/om200069t