(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

Base Information

Chemical Name:(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2
CAS No.:105900-15-0
Molecular Formula:C₃₇H₄₂O₂P₂Zr
Molecular Weight:671.911
Hs Code.:

(C<sub>5</sub>(CH<sub>3</sub>)5)Zr(CH<sub>3</sub>)(OCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

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Chemical Property of (C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

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Technology Process of (C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

There total 1 articles about (C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: Cp(*)ZrMe₃

: 5958-44-1
diphenylphosphinomethanol

: 105900-15-0
(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

Guidance literature:: With air; In hexane; byproducts: CH4; addn. of Zr complex to a slurry of HOCH2PPh2 in hexane, addn. of more hexane; reaction mixture is placed under Ar, and a small amount of air is allowed to diffuse into the flask.; elem. anal.;

Reference yield: 75.0%

: di(rhodium)tetracarbonyl dichloride

: 105900-15-0
(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

: 105900-16-1
(CH3)5CpZr(μ-OCH2Ph2P)2(μ2-η2-OC(CH3))(μ-Cl)RhCO

Guidance literature:: In toluene; 25°C; elem. anal.;
DOI:10.1021/ja00286a045

Reference yield: 75.0%

: 105900-15-0
(C₅(CH₃)5)Zr(CH₃)(OCH₂P(C₆H₅)2)2

: 15320-81-7
[(triphenylphosphine)3Rh(CH₃)]

: 114995-18-5
cis-(CH3)5CpZr(μ-OCH2Ph2P)2RhMe2

Guidance literature:: In toluene; byproducts: PPh3; To a flask contg. Zr and Rh complexes is distilled toluene at -78°C, stirred for 5 min at that temp., for 20 min at 0°C, and for 1.5 h at 25°C.; removal of solvent, trituration with hexane, filtn., washing with hexane, drying in vacuo; elem. anal.;