4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

Base Information

Chemical Name:4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid
CAS No.:170799-57-2
Molecular Formula:C₁₈H₂₃N₅O₂
Molecular Weight:341.413
Hs Code.:

4-<N-<2-(2,4-diamino-6,7-dihydro-5H-cyclopenta<d>pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

Synonyms:4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

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Chemical Property of 4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

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Technology Process of 4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

There total 10 articles about 4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 170799-63-0
ethyl 4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoate

: 170799-57-2
4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1248/cpb.43.829

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 170799-57-2
4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

Guidance literature:: Multi-step reaction with 10 steps

1: 87 percent / N,N-diisopropylethylamine / dimethylformamide / 24 h / 70 °C

2: 82 percent / NaHCO₃

3: 97 percent / 1N NaOH

4: 58 percent / BH₃ / tetrahydrofuran

5: Et₃N

6: NaI

7: BuSnH, AIBN / benzene / Heating

8: iso-Pr₂EtN

9: 67 percent

10: 96 percent / 1N HCl / acetic acid

With hydrogenchloride; sodium hydroxide; n-butyl tin hydride; 2,2'-azobis(isobutyronitrile); borane; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.43.829

Reference yield:

: 170799-73-2
ethyl 4-benzoate

: 170799-57-2
4-pyrimidin-5-yl)ethyl>-N-ethylamino>benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: BuSnH, AIBN / benzene / Heating

2: iso-Pr₂EtN

3: 67 percent

4: 96 percent / 1N HCl / acetic acid

With hydrogenchloride; n-butyl tin hydride; 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; In acetic acid; benzene;
DOI:10.1248/cpb.43.829