C₁₇H₁₈N₂O₄

Base Information

• Chemical Name: C₁₇H₁₈N₂O₄
• CAS No.: 958633-81-3
• Molecular Formula: C₁₇H₁₈N₂O₄
• Molecular Weight: 314.341
• Mol file: 958633-81-3.mol

Synonyms:C₁₇H₁₈N₂O₄

Chemical Property of C₁₇H₁₈N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈N₂O₄

There total 7 articles about C₁₇H₁₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Dictyoquinazol A (477203-69-3) → C17H18N2O4 (958633-81-3)

Guidance literature:

Dictyoquinazol A; With oxalyl dichloride; In chloroform; for 1h; Heating;

With sodium cyanoborohydride; In tetrahydrofuran; at 20 ℃; for 6h; Further stages.;

DOI:10.1080/00397910701489537

Reference yield:

C16H16N2O5 (958633-72-2) → C17H18N2O4 (958633-81-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 100 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr

2.1: 100 percent / 1 h / Heating

3.1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / 24 h / 10 °C / Irradiation

3.2: 1.39 g / dimethylformamide / 24 h / 20 °C

4.1: 96 percent / sodium methoxide / methanol / 3 h / 20 °C

5.1: oxalyl chloride / CHCl₃ / 1 h / Heating

5.2: 100 percent / sodium cyanoborohydride / tetrahydrofuran / 6 h / 20 °C

With N-Bromosuccinimide; oxalyl dichloride; hydrogen; sodium methylate; dibenzoyl peroxide; palladium on activated charcoal; In methanol; tetrachloromethane; chloroform;

DOI:10.1080/00397910701489537

Reference yield:

5-methoxy-2-nitro-benzoic acid (1882-69-5) → C17H18N2O4 (958633-81-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: 77 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole; Et₃N / dimethylformamide / 5 h / 20 °C

2.1: 100 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr

3.1: 100 percent / 1 h / Heating

4.1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / 24 h / 10 °C / Irradiation

4.2: 1.39 g / dimethylformamide / 24 h / 20 °C

5.1: 96 percent / sodium methoxide / methanol / 3 h / 20 °C

6.1: oxalyl chloride / CHCl₃ / 1 h / Heating

6.2: 100 percent / sodium cyanoborohydride / tetrahydrofuran / 6 h / 20 °C

With N-Bromosuccinimide; oxalyl dichloride; hydrogen; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dibenzoyl peroxide; palladium on activated charcoal; In methanol; tetrachloromethane; chloroform; N,N-dimethyl-formamide;

DOI:10.1080/00397910701489537

upstream raw materials:

Dictyoquinazol A

C₁₆H₁₆N₂O₅

C₁₆H₁₈N₂O₃

6-methoxy-3-(4-methoxy-2-methylphenyl)quinazolin-4(3H)-one