bis(triphenylphosphine)gold(I) tetrafluoroborate

Base Information

Chemical Name:bis(triphenylphosphine)gold(I) tetrafluoroborate
CAS No.:25749-32-0
Molecular Formula:BF₄*C₃₆H₃₀AuP₂
Molecular Weight:808.353
Hs Code.:

Synonyms:bis(triphenylphosphine)gold(I) tetrafluoroborate

Suppliers and Price of bis(triphenylphosphine)gold(I) tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(triphenylphosphine)gold(I) tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(triphenylphosphine)gold(I) tetrafluoroborate

There total 23 articles about bis(triphenylphosphine)gold(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: tris(triphenylphosphinegold)cyclopentadiene fluoroborate

: 25749-32-0
bis(triphenylphosphine)gold(I) tetrafluoroborate

: C₅H₄(AuP(C₆H₅)3)2

Guidance literature:: With PPh₃; In acetone; to Au-complex in acetone added PPh3 in acetone, mixture held for 10 h at 0°C; separated, washed with acetone, ethanol and ether, dried in vac., mother soln. and wash soln. combined, evaporated to dryness, residue washed with ether, recrystd. from ethanol-ether-petroleum ether; elem. anal.;

Reference yield: 98.0%

: tetrafluoroboric acid

: tetraphenylcyclopentadienyl(triphenylphosphine)gold

: 25749-32-0
bis(triphenylphosphine)gold(I) tetrafluoroborate

: tetraphenylcyclopentadiene

Guidance literature:: With PPh₃; In tetrahydrofuran; diethyl ether; to a soln. of Au-complex and PPh3 in THF added soln. of HBF4 in ether dropwise; filtered, washed with benzene and ether, filtrate evaporated to drynessin vac., residue dissolved in benzene, with the aid of petroleum ether precipitated organic compound from benzene soln.;

Reference yield: 98.0%

: tetrafluoroboric acid

: tetraphenylcyclopentadienyl(triphenylphosphine)gold(I)

: 603-35-0
triphenylphosphine

: 25749-32-0
bis(triphenylphosphine)gold(I) tetrafluoroborate

Guidance literature:: In tetrahydrofuran; byproducts: tetraphenylcyclopentadiene; soln. of HBF4 in ether was added dropwise to soln. of Au complex and PPh3 in THF; crystalline ppt. filtered, washed with benzene and ether, crystn. from methanol, hexane, ether;
DOI:10.1016/S0022-328X(00)93456-9