C₅₂H₅₃N₅O₉S

Base Information

Chemical Name:C₅₂H₅₃N₅O₉S
CAS No.:1371641-92-7
Molecular Formula:C₅₂H₅₃N₅O₉S
Molecular Weight:924.087
Hs Code.:

C<sub>52</sub>H<sub>53</sub>N<sub>5</sub>O<sub>9</sub>S

Synonyms:C₅₂H₅₃N₅O₉S

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Chemical Property of C₅₂H₅₃N₅O₉S

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Technology Process of C₅₂H₅₃N₅O₉S

There total 7 articles about C₅₂H₅₃N₅O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1371641-86-9
C₅₁H₅₁N₅O₇

: 7143-01-3
Methanesulfonic anhydride

: 1371641-92-7
C₅₂H₅₃N₅O₉S

Guidance literature:: With triethylamine; In dichloromethane; at 23 ℃; for 2h;

Reference yield:

: 1253799-75-5
((4aS,8S,8aR,9S)-8-azido-3-(benzyloxy)-4a-((tert-butyldimethylsilyl)oxy)-9-(dimethylamino)-8a,9-dihydronaphtho[2,3-d]isoxazole-4,5(4aH,8H)-dione)

: 1371641-92-7
C₅₂H₅₃N₅O₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - -10 °C

1.3: pH 7 / Aqueous potassium phosphate buffer

2.1: hydrogen fluoride / acetonitrile; water / 13 h / 23 °C

3.1: trimethylphosphane / toluene; benzene / 0.33 h / 23 °C

3.2: 2 h / 23 °C

4.1: triethylamine / dichloromethane / 2 h / 23 °C

With N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; triethylamine; lithium diisopropyl amide; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; benzene; 1.2: Michael-Claisen cyclization;

Reference yield:

: 1371641-83-6
C₅₇H₆₃N₇O₇Si

: 1371641-92-7
C₅₂H₅₃N₅O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen fluoride / acetonitrile; water / 13 h / 23 °C

2.1: trimethylphosphane / toluene; benzene / 0.33 h / 23 °C

2.2: 2 h / 23 °C

3.1: triethylamine / dichloromethane / 2 h / 23 °C

With hydrogen fluoride; triethylamine; trimethylphosphane; In dichloromethane; water; toluene; acetonitrile; benzene;