C₁₆H₁₅BrO₄

Base Information

• Chemical Name: C₁₆H₁₅BrO₄
• CAS No.: 1334670-02-8
• Molecular Formula: C₁₆H₁₅BrO₄
• Molecular Weight: 351.197
• Mol file: 1334670-02-8.mol

Synonyms:C₁₆H₁₅BrO₄

Chemical Property of C₁₆H₁₅BrO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₅BrO₄

There total 1 articles about C₁₆H₁₅BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C13H13BrO4 (1236112-80-3) + propargyl bromide (106-96-7) → C16H15BrO4 (1334670-02-8)

Guidance literature:

C₁₃H₁₃BrO₄; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h;

propargyl bromide; In N,N-dimethyl-formamide; toluene; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201101917

Reference yield: 69.0%

C16H15BrO4 (1334670-02-8) + Bis(trimethylsilyl)ethyne (14630-40-1) → C24H32O4Si2 (1334669-77-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; acetonitrile; at 120 ℃; Microwave irradiation;

DOI:10.1002/chem.201101917

Reference yield: 65.0%

hex-3-yne (928-49-4) + C16H15BrO4 (1334670-02-8) → C22H24O4 (1334669-76-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; acetonitrile; at 120 ℃; Microwave irradiation;

DOI:10.1002/chem.201101917

upstream raw materials:

C₁₃H₁₃BrO₄

propargyl bromide

Downstream raw materials:

C₂₂H₂₄O₄

C₂₄H₃₂O₄Si₂