P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

Base Information

Chemical Name:P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene
CAS No.:347192-81-8
Molecular Formula:C₁₇H₂₀NO₂P
Molecular Weight:301.325
Hs Code.:

Synonyms:P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

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Chemical Property of P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

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Technology Process of P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

There total 2 articles about P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 127802-82-8
P-(ethyl)-P,P-(diphenyl)(N-methoxycarbonyl)phosphazene

: 347192-81-8
P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

Guidance literature:: P-(ethyl)-P,P-(diphenyl)(N-methoxycarbonyl)phosphazene; With n-butyllithium; In tetrahydrofuran; hexane; at -30 ℃; for 0.5h;

methyl halide; In tetrahydrofuran; hexane; at -70 - 25 ℃;
DOI:10.1016/S0040-4020(01)00165-X

Reference yield:

: 607-01-2
ethyl-diphenyl-phosphane

: 347192-81-8
P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane

2.1: n-butyllithium / tetrahydrofuran / -30 °C / Inert atmosphere; Schlenk technique

2.2: -70 - 20 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In tetrahydrofuran; dichloromethane; 1.1: |Staudinger Azide Reduction;
DOI:10.1055/a-1644-2806

Reference yield: 100.0%

: 347192-81-8
P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene

: 74-88-4
methyl iodide

: 2-(tert-butyl-phenyl-phosphinoyl)-benzamide

Guidance literature:: P,P-diphenyl-P-(1-methylethyl)(N-methoxycabonyl)phosphazene; With tert.-butyl lithium; In tetrahydrofuran; at -35 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at -95 ℃; for 2.5h;

With hydrogenchloride; In tetrahydrofuran; for 0.5h;
DOI:10.1039/b212708c