Technology Process of C30H35N7O10S2
There total 6 articles about C30H35N7O10S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C63H76N7O15S2(1+)*I(1-);
With
aluminum (III) chloride;
In
nitromethane; dichloromethane; methoxybenzene;
at -40 - 0 ℃;
for 0.833333h;
With
hydrogenchloride;
In
diethyl ether; nitromethane; dichloromethane; water; methoxybenzene; acetonitrile;
at -40 - 0 ℃;
for 1h;
With
phosphorus tribromide;
In
dichloromethane; N,N-dimethyl-formamide;
at 0 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / platinum(IV) oxide / dichloromethane; ethyl acetate / 2 h
2.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 1 h / -15 °C
2.2: -15 - 20 °C
3.1: N,N-dimethyl-formamide / 3 h / 20 °C
3.2: 1 h / -40 - 0 °C
3.3: 0.5 h / 0 °C
4.1: aluminum (III) chloride / dichloromethane; nitromethane; methoxybenzene / 0.83 h / -40 - 0 °C
4.2: 1 h / -40 - 0 °C
4.3: 0.5 h / 0 °C
With
aluminum (III) chloride; hydrogen; methanesulfonyl chloride; triethylamine;
platinum(IV) oxide;
In
nitromethane; dichloromethane; N,N-dimethyl acetamide; ethyl acetate; methoxybenzene; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 1 h / -15 °C
1.2: -15 - 20 °C
2.1: N,N-dimethyl-formamide / 3 h / 20 °C
2.2: 1 h / -40 - 0 °C
2.3: 0.5 h / 0 °C
3.1: aluminum (III) chloride / dichloromethane; nitromethane; methoxybenzene / 0.83 h / -40 - 0 °C
3.2: 1 h / -40 - 0 °C
3.3: 0.5 h / 0 °C
With
aluminum (III) chloride; methanesulfonyl chloride; triethylamine;
In
nitromethane; dichloromethane; N,N-dimethyl acetamide; methoxybenzene; N,N-dimethyl-formamide;