(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

Base Information

Chemical Name:(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one
CAS No.:1571062-19-5
Molecular Formula:C₂₁H₂₆ClNO₅
Molecular Weight:407.894
Hs Code.:

Synonyms:(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

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Chemical Property of (E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

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Technology Process of (E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

There total 6 articles about (E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616931-18-0
C₁₆H₂₁ClO₄

: 207976-92-9
3-chloro-5,6-dihydro-1H-pyridin-2-one

: 1571062-19-5
(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.05.070

Reference yield:

: 675-20-7
piperidin-2-one

: 1571062-19-5
(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus pentachloride / chloroform / 3.25 h / 0 °C / Reflux

2: lithium carbonate / N,N-dimethyl-formamide / 7 h / 120 °C

3: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With phosphorus pentachloride; lithium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.05.070

Reference yield:

: 1571062-39-9
(E)-2-butyl-3-(3,4,5-trimethoxyphenyl)acrylic acid

: 1571062-19-5
(E)-3-chloro-1-(2-butyl-3-(3,4,5-trimethoxyphenyl)acryloyl)-5,6-dihydropyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

1.2: 0.25 h / 0 °C / Reflux; Inert atmosphere

2.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With oxalyl dichloride; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2014.05.070