Technology Process of C26H23NO6
There total 3 articles about C26H23NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H23NO5;
With
sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
tetrahydrofuran; water; tert-butyl alcohol;
at 15 ℃;
With
sodium chlorite;
In
tetrahydrofuran; water; tert-butyl alcohol;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
2: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 18.5 h / -15 - 20 °C / Inert atmosphere
3: ozone / dichloromethane / -70 °C
4: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 10 - 20 °C
With
pyridine; sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; ozone;
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; dichloromethane; water; isopropyl alcohol; mineral oil; tert-butyl alcohol;
4: Pinnick Oxidation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 18.5 h / -15 - 20 °C / Inert atmosphere
2: ozone / dichloromethane / -70 °C
3: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 10 - 20 °C
With
sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; ozone;
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; dichloromethane; water; mineral oil; tert-butyl alcohol;
3: Pinnick Oxidation;