1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Base Information

Chemical Name:1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane
CAS No.:1071149-50-2
Molecular Formula:C₄₈H₅₀Cl₂N₂P₂
Molecular Weight:787.792
Hs Code.:

Synonyms:1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

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Chemical Property of 1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

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Technology Process of 1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

There total 9 articles about 1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1257432-58-8
[2,6-bis-(2,4,6-trimethylphenyl)phenyl]amino(dichloro)phosphane

: 1071149-50-2
1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Guidance literature:: With triethylamine; In hexane; at -80 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0dt00700e

Reference yield: 20.0%

: dimethylsulfide gold(I) chloride

: 1338063-88-9
2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

: 1071149-50-2
1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

: C₄₈H₅₀AuClN₂P₂

: C₄₈H₅₀Au₂Cl₂N₂P₂

Guidance literature:: In benzene; at 20 ℃; for 1h;
DOI:10.1039/c6cc01935h

Reference yield:

: 103068-13-9
2,4,6,2'',4'',6''-hexamethyl-1,1':3',1''-terphenyl

: 1071149-50-2
1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Guidance literature:: Multi-step reaction with 5 steps

1.1: iodine / tetrahydrofuran / 11 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether / 1.5 h / 0 °C / Inert atmosphere

2.2: 2.25 h / 0 - 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 3.33 h / -60 °C / Inert atmosphere; Reflux

4.1: phosphorus trichloride / diethyl ether / 0.08 h / -40 °C / Inert atmosphere

4.2: -40 - 20 °C / Inert atmosphere

5.1: triethylamine / hexane / -80 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; iodine; triethylamine; phosphorus trichloride; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1039/c0dt00700e