2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Base Information

• Chemical Name: 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane
• CAS No.: 1338063-88-9
• Molecular Formula: C₄₈H₅₀N₂P₂
• Molecular Weight: 716.886
• Mol file: 1338063-88-9.mol

Synonyms:2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Chemical Property of 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane

There total 4 articles about 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane (1071149-50-2) → 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane (1338063-88-9)

Guidance literature:

With magnesium; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.201403964

Reference yield:

C61H58N2OP2S → 9H-xanthene-9-thione (492-21-7) + 2,4-bis[2,6-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane (1338063-88-9)

Guidance literature:

With hydrogen; In toluene; at 25 ℃; for 0.833333h; Schlenk technique;

DOI:10.1021/acs.inorgchem.1c03207

Reference yield:

C58H68N4P2 → [P(μ-NTer)]2 (1338063-88-9) + C53H63N3P2

Guidance literature:

Inert atmosphere;

DOI:10.1039/c8sc04893b

upstream raw materials:

1,3-dichloro-2,4-bis[2,4-bis(2,4,6-trimethylphenyl)phenyl]-1,3-diphospha-2,4-diazacyclobutane