(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

Base Information

Chemical Name:(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester
CAS No.:914645-12-8
Molecular Formula:C₂₁H₃₂N₂O₂
Molecular Weight:344.497
Hs Code.:

Synonyms:(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

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Chemical Property of (S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

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Technology Process of (S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

There total 5 articles about (S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 914645-11-7
(S)-{[4-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl]-amino}-phenyl-acetic acid cyclopentyl ester

: 914645-12-8
(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 162046-58-4
4-(N-tert-butyloxycarbonylaminomethyl)-cyclohexane-1-carboxylic acid

: 914645-12-8
(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 0 - 20 °C

2.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

3.1: 1,1-dichloroethane / 0.42 h / 20 °C

3.2: 1.5 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With lithium aluminium tetrahydride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane;

Reference yield:

: tranexamic acid

: 914645-12-8
(S)-[(4-aminomethyl-cyclohexylmethyl)-amino]-phenyl-acetic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 5 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

4.1: 1,1-dichloroethane / 0.42 h / 20 °C

4.2: 1.5 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With sodium hydroxide; lithium aluminium tetrahydride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane; water;