2-Iodoterephthalaldehyde

Base Information

Chemical Name:2-Iodoterephthalaldehyde
CAS No.:385416-64-8
Molecular Formula:C8H5 I O2
Molecular Weight:260.03
Hs Code.:
DSSTox Substance ID:DTXSID20709104
Wikidata:Q82643847
Mol file:385416-64-8.mol

Synonyms:2-Iodoterephthalaldehyde;385416-64-8;2-Iodo-1,4-benzenedicarboxaldehyde;1,4-Benzenedicarboxaldehyde,2-iodo-;DTXSID20709104;2-iodobenzene-1,4-dicarbaldehyde

Suppliers and Price of 2-Iodoterephthalaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-IODO-1,4-BENZENEDICARBOXALDEHYDE 98.00%
5MG
$ 496.33

Total 5 raw suppliers

Chemical Property of 2-Iodoterephthalaldehyde

Chemical Property:

PSA：34.14000
LogP:1.91620
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:259.93343
Heavy Atom Count:11
Complexity:158

Purity/Quality:

99% ^*data from raw suppliers

2-IODO-1,4-BENZENEDICARBOXALDEHYDE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C=O)I)C=O

Technology Process of 2-Iodoterephthalaldehyde

There total 6 articles about 2-Iodoterephthalaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: (2-iodo-1,4-phenylene)dimethanol

: 385416-64-8
2-iodo-1,4-benzenedicarboxaldehyde

: 4-hydroxymethyl-2-iodobenzaldehyde

: 4-(hydroxymethyl)-3-iodobenzaldehyde

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Solvent; Temperature;
DOI:10.1016/j.tet.2019.130765

Reference yield:

: (2-iodo-1,4-phenylene)dimethanol

: 385416-64-8
2-iodo-1,4-benzenedicarboxaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo0105540

Reference yield:

: 165534-79-2
dimethyl 2-iodoterephthalate

: 385416-64-8
2-iodo-1,4-benzenedicarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL-H / various solvent(s); tetrahydrofuran / 6 h / -78 °C

2: 0.53 g / PCC / CH₂Cl₂ / 24 h / 20 °C

With diisobutylaluminium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0105540