C₂₄H₄₀N₂O₇SiS

Base Information

Chemical Name:C₂₄H₄₀N₂O₇SiS
CAS No.:937204-24-5
Molecular Formula:C₂₄H₄₀N₂O₇SSi
Molecular Weight:528.742
Hs Code.:

C<sub>24</sub>H<sub>40</sub>N<sub>2</sub>O<sub>7</sub>SiS

Synonyms:C₂₄H₄₀N₂O₇SiS

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Chemical Property of C₂₄H₄₀N₂O₇SiS

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Technology Process of C₂₄H₄₀N₂O₇SiS

There total 5 articles about C₂₄H₄₀N₂O₇SiS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 937203-86-6
(R)-2-((R)-1-(triethylsilyloxy)ethyl)but-3-en-1-ol

: 552847-32-2
tert-butyl 2-[(2-nitrobenzene)sulfonamido]acetate

: 937204-24-5
C₂₄H₄₀N₂O₇SiS

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 70 ℃; for 0.5h;
DOI:10.1021/ol0631197

Reference yield:

: 937204-09-6
C₂₂H₃₃NO₄Si

: 937204-24-5
C₂₄H₄₀N₂O₇SiS

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / methanol; LiBH₄ / diethyl ether / 3 h / 0 - 20 °C

2: 80 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 0.5 h / 70 °C

With methanol; lithium borohydride; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ol0631197

Reference yield:

: 937203-85-5
C₁₆H₁₉NO₄

: 937204-24-5
C₂₄H₄₀N₂O₇SiS

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / dimethylformamide / 4 h / 20 °C

2: 84 percent / methanol; LiBH₄ / diethyl ether / 3 h / 0 - 20 °C

3: 80 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 0.5 h / 70 °C

With 1H-imidazole; methanol; lithium borohydride; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; N,N-dimethyl-formamide; toluene; 3: Mitsunobu reaction;
DOI:10.1021/ol0631197