5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

Base Information

• Chemical Name: 5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one
• CAS No.: 1392411-82-3
• Molecular Formula: C₁₇H₁₉FN₄O₃
• Molecular Weight: 346.361

Synonyms:5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

Chemical Property of 5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

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Technology Process of 5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

There total 1 articles about 5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-benzyl-5-(2,2-diethoxyethyl)-1H-pyrazolo-[3,4-d]pyrimidin-4(5H)-one (289651-72-5) + chloroacetaldehyde diethyl acetal (621-62-5) → 5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (1392411-82-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; for 7h; Reflux;

DOI:10.1134/S1070428012070172

Reference yield: 95.0%

5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (1392411-82-3) → 5-amino-N-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazole-4-carboxamide (1234320-78-5)

Guidance literature:

With sodium hydroxide; In ethanol; for 5h; Reflux;

DOI:10.1134/S1070428012070172

Reference yield: 91.0%

5-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (1392411-82-3) → 2-[5-amino-1-(4-fluorophenyl)-1H-pyrazol-4-ylcarbonylamino]acetic acid (1234320-72-9)

Guidance literature:

With sodium hydroxide; In ethanol; for 5h; Reflux;

DOI:10.1134/S1070428012070172

upstream raw materials:

1-benzyl-5-(2,2-diethoxyethyl)-1H-pyrazolo-[3,4-d]pyrimidin-4(5H)-one

chloroacetaldehyde diethyl acetal

Downstream raw materials:

5-amino-N-(2,2-diethoxyethyl)-1-(4-fluorophenyl)-1H-pyrazole-4-carboxamide

1-(4-fluorophenyl)-7-hydroxy-5,6,7,8-tetrahydropyrazolo[3,4-e][1,4]diazepin-4(1H)-one

2-[5-amino-1-(4-fluorophenyl)-1H-pyrazol-4-ylcarbonylamino]acetic acid

1-(4-fluorophenyl)-1,5,6,8-tetrahydropyrazolo-[3,4-e][1,4]diazepine-4,7-dione

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