2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

Base Information

Chemical Name:2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione
CAS No.:958463-37-1
Molecular Formula:C₂₃H₂₉NO₄SSi
Molecular Weight:443.639
Hs Code.:

Synonyms:2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

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Chemical Property of 2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

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Technology Process of 2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

There total 8 articles about 2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 54974-07-1
phthalimidesulfenyl chloride

: C₁₅H₂₆O₃Si

: 958463-37-1
2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

Guidance literature:: In chloroform; for 5h;
DOI:10.1002/chem.200700309

Reference yield: 91.0%

: 54974-07-1
phthalimidesulfenyl chloride

: 112136-00-2
4-(tert-butyldimethylsilyloxy)-2,3,5-trimethylphenol

: 958463-37-1
2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 958463-37-1
2-((3-((t-butyldimethylsilyl)oxy)-6-hydroxy-2,4,5-trimethylphenyl)thio)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 24 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.42 h / 0 °C

4: dichloromethane / 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;