Technology Process of 2-(4-methoxyphenyl)butane 1,4-dimesylate
There total 5 articles about 2-(4-methoxyphenyl)butane 1,4-dimesylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; TEA;
In
dichloromethane;
at 25 ℃;
for 6h;
DOI:10.1021/jm990428c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 52 percent / K2CO3 / methanol / 24 h / Heating
2: 71 percent / conc. H2SO4 / 5 h / Heating
3: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h / 25 °C / 760.05 Torr
4: 69 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
5: 94 percent / TEA; DMAP / CH2Cl2 / 6 h / 25 °C
With
dmap; lithium aluminium tetrahydride; TEA; sulfuric acid; hydrogen; potassium carbonate;
10percent Pd/C;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
1: Dean and Blum procedure / 2: ethanolysis / 3: Catalytic hydrogenation / 4: Reduction / 5: mesylation;
DOI:10.1021/jm990428c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h / 25 °C / 760.05 Torr
2: 69 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
3: 94 percent / TEA; DMAP / CH2Cl2 / 6 h / 25 °C
With
dmap; lithium aluminium tetrahydride; TEA; hydrogen;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane;
1: Catalytic hydrogenation / 2: Reduction / 3: mesylation;
DOI:10.1021/jm990428c
