Technology Process of C18H26N2O
There total 5 articles about C18H26N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Wilkinson's catalyst;
In
1,4-dioxane;
at 130 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/ja306123m
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Wilkinson's catalyst / 1,4-dioxane / 24 h / 130 °C / 760 Torr / Inert atmosphere
2: hydrogenchloride; acetic acid / water / 24 h / 120 °C / Inert atmosphere; Sealed tube
3: aluminum oxide / toluene / 36 h / Inert atmosphere; Molecular sieve; Reflux
4: Wilkinson's catalyst / 1,4-dioxane / 24 h / 130 °C / Inert atmosphere
With
hydrogenchloride; aluminum oxide; Wilkinson's catalyst; acetic acid;
In
1,4-dioxane; water; toluene;
DOI:10.1021/ja306123m
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; acetic acid / water / 24 h / 120 °C / Inert atmosphere; Sealed tube
2: aluminum oxide / toluene / 36 h / Inert atmosphere; Molecular sieve; Reflux
3: Wilkinson's catalyst / 1,4-dioxane / 24 h / 130 °C / Inert atmosphere
With
hydrogenchloride; aluminum oxide; Wilkinson's catalyst; acetic acid;
In
1,4-dioxane; water; toluene;
DOI:10.1021/ja306123m