5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:161762-07-8
Molecular Formula:C₄₀H₄₇NO₈
Molecular Weight:669.815
Hs Code.:

Synonyms:5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of 5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 7 articles about 5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 161762-05-6
5-<(benzyloxycarbonyl)amino>pentyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 161762-07-8
5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; diethyl ether; 3 A molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1016/S0008-6215(05)80010-2

Reference yield:

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: 161762-07-8
5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / Ag₂CO₃, CaSO₄ / CHCl₃ / 20 h / Ambient temperature

2: 63 percent / NaOMe / methanol / 24 h / Ambient temperature

3: 88 percent / ZnCl₂ / 192 h / Ambient temperature

4: 77 percent / KOH / dimethylformamide / 1 h / 0 °C

5: 70 percent / NaBH₃CN, HCl/Et₂O, mol. sieves 3A / tetrahydrofuran / Ambient temperature

With hydrogenchloride; calcium sulfate; potassium hydroxide; diethyl ether; 3 A molecular sieve; sodium methylate; sodium cyanoborohydride; silver carbonate; zinc(II) chloride; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(05)80010-2

Reference yield:

: 100-52-7
benzaldehyde

: 161762-07-8
5-<(benzyloxycarbonyl)amino>pentyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / ZnCl₂ / 192 h / Ambient temperature

2: 77 percent / KOH / dimethylformamide / 1 h / 0 °C

3: 70 percent / NaBH₃CN, HCl/Et₂O, mol. sieves 3A / tetrahydrofuran / Ambient temperature

With hydrogenchloride; potassium hydroxide; diethyl ether; 3 A molecular sieve; sodium cyanoborohydride; zinc(II) chloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(05)80010-2