tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside
• CAS No.: 1235137-62-8
• Molecular Formula: C₅₃H₅₆Cl₃NO₁₃S
• Molecular Weight: 1053.45
• Mol file: 1235137-62-8.mol

Synonyms:tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside

Chemical Property of tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside

There total 1 articles about tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-O-benzyl-4,6-O-benzylidene-3-O-(p-methoxybenzyl)-D-mannopyranosyl trichloroacetimidate + tolyl 3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (502692-38-8) → p-tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-thio-α-D-mannopyranoside (1071226-08-8) + N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide (1235137-12-8) + tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (1235137-09-3) + tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (1235137-62-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -50 ℃; Molecular sieve; Inert atmosphere;

DOI:10.1002/asia.200900765

upstream raw materials:

tolyl 3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside