methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

Base Information

Chemical Name:methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate
CAS No.:1203507-08-7
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

Suppliers and Price of methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

There total 1 articles about methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-07-2
4-methoxy-benzoyl chloride

: 7682-18-0
methyl 2-aminobutanoate hydrochloride

: 1203507-08-7
methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200904333

Reference yield: 100.0%

: 1203507-08-7
methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

: 217446-32-7
DL-(N-(4-methoxybenzoyl))-2-aminobutyric acid

Guidance literature:: methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate; With water; sodium hydroxide; In methanol; at 20 ℃; for 1h;

With hydrogenchloride; In water;
DOI:10.1002/anie.200904333

Reference yield:

: 1203507-08-7
methyl DL-(N-(4-methoxybenzoyl))-2-aminobutanoate

: (R,E)-tert-butyl 4-(4-ethyl-2-(4-methoxyphenyl)-5-oxo-4,5-dihydrooxazol-4-yl)but-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol

2: dicyclohexyl-carbodiimide / dichloromethane / 20 °C

3: N-((2S,3R)-3-(tert-butyldiphenylsilyloxy)-1-(diphenylphosphino)butan-2-yl)-4-methylbenzenesulfonamide / toluene / 20 °C / Inert atmosphere

With N-((2S,3R)-3-(tert-butyldiphenylsilyloxy)-1-(diphenylphosphino)butan-2-yl)-4-methylbenzenesulfonamide; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; toluene;
DOI:10.1021/jacs.5b10524