(3-Cyano)-4-picolylacetat

Base Information

• Chemical Name: (3-Cyano)-4-picolylacetat
• CAS No.: 157650-26-5
• Molecular Formula: C₉H₈N₂O₂
• Molecular Weight: 176.175
• Mol file: 157650-26-5.mol

Synonyms:(3-Cyano)-4-picolylacetat

Chemical Property of (3-Cyano)-4-picolylacetat

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (3-Cyano)-4-picolylacetat

There total 1 articles about (3-Cyano)-4-picolylacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-cyano-4-methylpyridine (5444-01-9) → (3-Cyano)-4-picolylacetat (157650-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / 30percent H₂O₂ / acetic acid / 1.) 80 deg C, 3 h, 2.) 70-80 deg C, 13 h

2: 21 percent / 0.08 h / 140 °C

With dihydrogen peroxide; In acetic acid;

DOI:10.1002/ardp.19943270814

Reference yield:

(3-Cyano)-4-picolylacetat (157650-26-5) → 3-Cyano-4-hydroxymethylpyridin (157650-27-6)

Guidance literature:

With potassium carbonate; In methanol; water; for 5h; Yield given; Ambient temperature;

DOI:10.1002/ardp.19943270814

upstream raw materials:

3-cyano-4-methylpyridine

Downstream raw materials:

3-Cyano-4-hydroxymethylpyridin

Refernces