(E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol

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Chemical Name:(E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol
CAS No.:1352457-93-2
Molecular Formula:C₁₇H₂₂NO₃
Molecular Weight:288.367
Hs Code.:

Synonyms:(E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol

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Chemical Property of (E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol

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Technology Process of (E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol

There total 1 articles about (E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 69971-72-8
1-oxyl-4-vinyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine

: 167764-53-6
(diacetoxyiodo)benzene diacetate

: 1352457-93-2
(E)-5-(2-(1-oxyl-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-4-yl)vinyl)benzene-1,3-diol

Guidance literature:: 1-oxyl-4-vinyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine; (diacetoxyiodo)benzene diacetate; With tetrabutylammomium bromide; potassium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h; Inert atmosphere;

With sodium methylate; In methanol; at 20 ℃; for 1h; diastereospecific reaction;
DOI:10.1016/j.bmc.2011.10.066