(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

Base Information

Chemical Name:(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane
CAS No.:1415456-25-5
Molecular Formula:C₂₄H₄₀O₄
Molecular Weight:392.579
Hs Code.:

Synonyms:(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

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Chemical Property of (2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

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Technology Process of (2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

There total 4 articles about (2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1415456-08-4
1,5-dimethoxy-6-(3-methylbut-2-en-1-yl)cyclohexa-1,4-diene

: 1415456-24-4
(2S,3R)-3-(bromomethyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

: 1415456-25-5
(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

Guidance literature:: 1,5-dimethoxy-6-(3-methylbut-2-en-1-yl)cyclohexa-1,4-diene; With sec.-butyllithium; In cyclohexane; at -78 - -30 ℃; for 0.75h;

(2S,3R)-3-(bromomethyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane; In tetrahydrofuran; cyclohexane; at -78 - 0 ℃; for 3.5h;

Reference yield:

: 503-60-6
3,3-dimethyl-allyl chloride

: 1415456-25-5
(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; barium(II) iodide / pentane; tetrahydrofuran / 1 h / -78 °C

1.2: 2.25 h

2.1: sec.-butyllithium / cyclohexane / 0.75 h / -78 - -30 °C

2.2: 3.5 h / -78 - 0 °C

With barium(II) iodide; tert.-butyl lithium; sec.-butyllithium; In tetrahydrofuran; cyclohexane; pentane;

Reference yield:

: 37567-78-5
1,5-dimethoxy-1,4-cyclohexadiene

: 1415456-25-5
(2S,3S)-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-(4-methoxy-4-methylpentyl)-2-methyloxirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; barium(II) iodide / pentane; tetrahydrofuran / 1 h / -78 °C

1.2: 2.25 h

2.1: sec.-butyllithium / cyclohexane / 0.75 h / -78 - -30 °C

2.2: 3.5 h / -78 - 0 °C

With barium(II) iodide; tert.-butyl lithium; sec.-butyllithium; In tetrahydrofuran; cyclohexane; pentane;