C₁₅H₂₀O₅

Base Information

Chemical Name:C₁₅H₂₀O₅
CAS No.:1453105-10-6
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>5</sub>

Synonyms:C₁₅H₂₀O₅

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Chemical Property of C₁₅H₂₀O₅

Chemical Property:

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Technology Process of C₁₅H₂₀O₅

There total 16 articles about C₁₅H₂₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1352234-58-2
(3aR,4aS,5S,8aS,8bR)-5-(benzyloxy)-2,2-dimethylhexahydro-[1,3]dioxolo[4,5-b]benzofuran-8a(4aH)-ol

: 1453105-10-6
C₁₅H₂₀O₅

Guidance literature:: With DOWEX 50W-8X ionic exchange resin; In 1,4-dioxane; water; for 72h;
DOI:10.1021/jo401166q

Reference yield:

: 1352234-51-5
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-β-L-arabinopentodialdofuranose

: 1453105-10-6
C₁₅H₂₀O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -78 °C

1.2: 3 h / -78 °C

2.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 23 °C

4.1: pyridinium chlorochromate; sodium acetate / dichloromethane / 6 h / 0 - 23 °C / Molecular sieve

5.1: palladium dichloride; copper diacetate; oxygen / water; N,N-dimethyl acetamide / 48 h

6.1: L-proline / N,N-dimethyl-formamide / 72 h / 20 °C

7.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 4 h / 0 - 20 °C

8.1: dmap / dichloromethane / 24 h / 23 °C

9.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.25 h / 110 °C

10.1: DOWEX 50W-8X ionic exchange resin / water; 1,4-dioxane / 72 h

With dmap; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; water; oxygen; tri-n-butyl-tin hydride; copper diacetate; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; palladium dichloride; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 1.1: |Sakurai Allylation / 1.2: |Sakurai Allylation / 9.1: |Barton-McCombie Deoxygenation;
DOI:10.1021/jo401166q

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
L-arabinose

: 1453105-10-6
C₁₅H₂₀O₅

Guidance literature:: Multi-step reaction with 15 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 60 °C

2.1: copper(II) sulfate; sulfuric acid / 1 h / 23 °C

3.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; tetrahydrofuran; mineral oil / 2 h / 0 - 23 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 23 °C

5.1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide; dichloromethane / 0.17 h / -20 °C

6.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -78 °C

6.2: 3 h / -78 °C

7.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 23 °C

9.1: pyridinium chlorochromate; sodium acetate / dichloromethane / 6 h / 0 - 23 °C / Molecular sieve

10.1: palladium dichloride; copper diacetate; oxygen / water; N,N-dimethyl acetamide / 48 h

11.1: L-proline / N,N-dimethyl-formamide / 72 h / 20 °C

12.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 4 h / 0 - 20 °C

13.1: dmap / dichloromethane / 24 h / 23 °C

14.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.25 h / 110 °C

15.1: DOWEX 50W-8X ionic exchange resin / water; 1,4-dioxane / 72 h

With 1H-imidazole; dmap; 2,2'-azobis(isobutyronitrile); sulfuric acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; oxygen; tri-n-butyl-tin hydride; copper diacetate; sodium acetate; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; sodium hydride; copper(II) sulfate; acetic acid; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; palladium dichloride; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 5.1: |Parikh-Doering Oxidation / 6.1: |Sakurai Allylation / 6.2: |Sakurai Allylation / 14.1: |Barton-McCombie Deoxygenation;
DOI:10.1021/jo401166q