(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Base Information

Chemical Name:(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium
CAS No.:1210405-61-0
Molecular Formula:C₂₂H₃₃HfI₃N₂
Molecular Weight:884.721
Hs Code.:

Synonyms:(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Suppliers and Price of (N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

There total 5 articles about (N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.7%

: (N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)-tris(phenylmethyl)hafnium

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1210405-61-0
(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 765-87-7
cyclohexane-1,2-dione

: 1210405-61-0
(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 5 h / Inert atmosphere; Reflux

2.1: toluene-4-sulfonic acid / toluene / 2 h / 80 °C / Inert atmosphere

3.1: titanium tetrachloride / toluene / 0.06 h / 20 - 49 °C / Inert atmosphere

3.2: 3.25 h / 20 °C / Inert atmosphere

4.1: toluene / 20 °C

5.1: dichloromethane / 0.5 h / 20 °C

With titanium tetrachloride; toluene-4-sulfonic acid; In dichloromethane; toluene;

Reference yield:

: 23740-64-9
2-morpholinocyclohex-2-enone

: 1210405-61-0
(N-((6E)-6-(butylimino-κN)-1-cyclohexen-1-yl)-2,6-bis(1-methylethyl)benzenaminato-κN)triiodohafnium

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 2 h / 80 °C / Inert atmosphere

2.1: titanium tetrachloride / toluene / 0.06 h / 20 - 49 °C / Inert atmosphere

2.2: 3.25 h / 20 °C / Inert atmosphere

3.1: toluene / 20 °C

4.1: dichloromethane / 0.5 h / 20 °C

With titanium tetrachloride; toluene-4-sulfonic acid; In dichloromethane; toluene;