ACETANILIDE-4'-D1

Base Information

• Chemical Name: ACETANILIDE-4'-D1
• CAS No.: 16625-79-9
• Molecular Formula: C8H8 D N O
• Molecular Weight: 136.17
• Mol file: 16625-79-9.mol

Synonyms:Acetanilide-4'-d(8CI)

Chemical Property of ACETANILIDE-4'-D1

Chemical Property:

• PSA: 29.10000
• LogP: 1.71800

Purity/Quality:

99% ^*data from raw suppliers

ACETANILIDE-4-D1 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ACETANILIDE-4'-D1

There total 4 articles about ACETANILIDE-4'-D1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-bromoacetanilide (103-88-8) → Essigsaeure-<4-D>anilid (16625-79-9)

Guidance literature:

With 1,10-Phenanthroline; carbon monoxide; water-d2; copper diacetate; triethylamine; at 120 ℃; for 48h; under 30003 Torr;

DOI:10.1039/d1sc04259a

Reference yield: 96.0%

N-(4-chlorophenyl)acetamide (539-03-7) → Essigsaeure-<4-D>anilid (16625-79-9)

Guidance literature:

With 1,2-propylene cyclic carbonate; water-d2; at 100 ℃; under 75007.5 Torr; chemoselective reaction; Flow reactor; Green chemistry;

DOI:10.1039/c8gc03192d

Reference yield: 30.0%

4-Acetamido-1-iodobenzene (622-50-4) → Essigsaeure-<4-D>anilid (16625-79-9)

Guidance literature:

With 1,2-propylene cyclic carbonate; water-d2; at 100 ℃; under 75007.5 Torr; chemoselective reaction; Flow reactor; Green chemistry;

DOI:10.1039/c8gc03192d

upstream raw materials:

N-(4-chlorophenyl)acetamide

4-Acetamido-1-iodobenzene

4-bromoacetanilide

Downstream raw materials:

4,4'-dideuterodiphenylamine