(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

Base Information

Chemical Name:(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol
CAS No.:191278-12-3
Molecular Formula:C₁₇H₂₄O
Molecular Weight:244.377
Hs Code.:

Synonyms:(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

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Chemical Property of (1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

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Technology Process of (1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

There total 7 articles about (1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 191278-17-8
(1S,8R,9R,10R)-8-phenyl-1-methylenedecalin oxide

: 191278-12-3
(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;
DOI:10.1021/jo970082i

Reference yield:

: 191530-46-8
(8R,9R,10R)-8-phenyl-1-decalone

: 191278-12-3
(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KOt-Bu / 1.) Et₂O, room temperature, 1 h, 2.) Et₂O, CH₂Cl₂, room temperature, 8 h

2: 1.) NBS, 2.) KOH / 1.) DME, H₂O, room temperature, 3 h, 2.) MeOH, H₂O, room temperature, 10 min

3: 84 percent / LiAlH₄ / diethyl ether / 1 h / Heating

With potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; potassium tert-butylate; In diethyl ether;
DOI:10.1021/jo970082i

Reference yield:

: 104197-81-1
(1S*,8R*,9R*,10R*)-8-phenyl-1-decalol

: 191278-12-3
(1S,8R,9R,10R)-1-methyl-8-phenyl-1-decalol

Guidance literature:: Multi-step reaction with 7 steps

1: 74 percent / pyridine / 4 h / Heating

2: 35 percent / diethyl cyanophosphate, Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temperature, 5 h

3: 89 percent / KOH / ethanol / 7 h / Heating

4: 91 percent / Jones reagent / acetone / 1 h / 0 °C

5: 1.) KOt-Bu / 1.) Et₂O, room temperature, 1 h, 2.) Et₂O, CH₂Cl₂, room temperature, 8 h

6: 1.) NBS, 2.) KOH / 1.) DME, H₂O, room temperature, 3 h, 2.) MeOH, H₂O, room temperature, 10 min

7: 84 percent / LiAlH₄ / diethyl ether / 1 h / Heating

With potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; jones reagent; diethyl cyanophosphonate; potassium tert-butylate; triethylamine; In pyridine; diethyl ether; ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo970082i