12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one

Base Information

• Chemical Name: 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one
• CAS No.: 82605-31-0
• Molecular Formula: C₂₄H₂₆N₂O
• Molecular Weight: 358.483

Synonyms:12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one

Chemical Property of 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one

There total 3 articles about 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Methyl-5-oxo-hexanoic acid [2-(1-benzyl-1H-indol-3-yl)-ethyl]-amide (82605-23-0) → 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one (82605-31-0)

Guidance literature:

With hydrogenchloride; In methanol; Heating;

DOI:10.1007/BF00762054

Reference yield:

N-benzyltryptamine (4307-98-6) → 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one (82605-31-0)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 22 h / Heating

2: 92 percent / aq. HCl / methanol / Heating

With hydrogenchloride; In methanol; benzene;

DOI:10.1007/BF00762054

Reference yield:

3,6-dimethyl-3,4-dihydro-2-pyrone (20155-55-9) → 12-Benzyl-3,12b-dimethyl-2,3,6,7,12,12b-hexahydro-1H-indolo[2,3-a]quinolizin-4-one (82605-31-0)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 22 h / Heating

2: 92 percent / aq. HCl / methanol / Heating

With hydrogenchloride; In methanol; benzene;

DOI:10.1007/BF00762054

upstream raw materials:

2-Methyl-5-oxo-hexanoic acid [2-(1-benzyl-1H-indol-3-yl)-ethyl]-amide

N-benzyltryptamine

3,6-dimethyl-3,4-dihydro-2-pyrone

Downstream raw materials:

STOCK₁N-05032

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