C₃₄H₂₆BF₂N₃

Base Information

• Chemical Name: C₃₄H₂₆BF₂N₃
• CAS No.: 1327339-74-1
• Molecular Formula: C₃₄H₂₆BF₂N₃
• Molecular Weight: 525.408
• Mol file: 1327339-74-1.mol

Synonyms:C₃₄H₂₆BF₂N₃

Chemical Property of C₃₄H₂₆BF₂N₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₄H₂₆BF₂N₃

There total 6 articles about C₃₄H₂₆BF₂N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

2-(4-methylphenyl)-4-phenyl-1H-pyrrole (1398056-91-1) + boron trifluoride diethyl etherate (109-63-7) → C34H26BF2N3 (1327339-74-1)

Guidance literature:

2-(4-methylphenyl)-4-phenyl-1H-pyrrole; With acetic anhydride; acetic acid; sodium nitrite; at 5 - 80 ℃; for 1h;

boron trifluoride diethyl etherate; With triethylamine; In 1,2-dichloro-ethane; at 20 - 80 ℃; for 1h;

Reference yield:

[5-(4-methylphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methylphenyl)-3-phenylpyrrol-2-ylidene]amine (1327339-71-8) → C34H26BF2N3 (1327339-74-1)

Guidance literature:

[5-(4-methylphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methylphenyl)-3-phenylpyrrol-2-ylidene]amine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.25h; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.2174/157017811796064377

Reference yield:

[5-(4-methylphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methylphenyl)-3-phenylpyrrol-2-ylidene]amine (1327339-71-8) + boron trifluoride (7637-07-2) → C34H26BF2N3 (1327339-74-1)

Guidance literature:

With triethylamine; In diethyl ether; 1,2-dichloro-ethane; at 20 - 80 ℃; for 1h;

DOI:10.1021/acs.jmedchem.0c00882

upstream raw materials:

[5-(4-methylphenyl)-3-phenyl-1H-pyrrol-2-yl][5-(4-methylphenyl)-3-phenylpyrrol-2-ylidene]amine

boron trifluoride

2-(4-methylphenyl)-4-phenyl-1H-pyrrole

boron trifluoride diethyl etherate