(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

Base Information

Chemical Name:(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine
CAS No.:189363-88-0
Molecular Formula:C₃₀H₃₃NO₂
Molecular Weight:439.598
Hs Code.:

Synonyms:(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

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Chemical Property of (S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

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Technology Process of (S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

There total 6 articles about (S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 90-99-3
diphenylchloromethane

: 189364-08-7
(S)-N-allyl-2-(3,4-dimethoxyphenyl)-2-cyclohexen-1-ylamine

: 189363-88-0
(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

Guidance literature:: With potassium carbonate; In various solvent(s); at 90 ℃; for 216h;
DOI:10.1021/jo9701187

Reference yield:

: 109380-07-6,109431-74-5,122797-27-7,61426-49-1
2-bromocyclohex-2-en-1-ol

: 189363-88-0
(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 2M Na₂CO₃, Pd(PPh₃)4, 2.) H₂O₂ / 1.) benzene, EtOH, 80 deg C, 1.3 h, 2.) room temperature, 1 h.

2: 99 percent / pyridine / CH₂Cl₂ / 3 h / Ambient temperature

3: (S)-BINAPO, Pd₂dba3*CHCl₃ / tetrahydrofuran / 19 h / Ambient temperature

4: 71 percent / sodium naphthalenide / tetrahydrofuran / 0.83 h / -78 °C

5: 45 percent / K₂CO₃ / various solvent(s) / 216 h / 90 °C

With pyridine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; sodium naphthalenide; sodium carbonate; potassium carbonate; (S)-1,1'-binaphthalene-2,2'-diylbis(diphenylphosphine oxide); In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo9701187

Reference yield:

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 189363-88-0
(S)-N-allyl-N-[2-(3,4-dimethoxyphenyl)-2-cyclohexenyl]diphenylmethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 2M Na₂CO₃, Pd(PPh₃)4, 2.) H₂O₂ / 1.) benzene, EtOH, 80 deg C, 1.3 h, 2.) room temperature, 1 h.

2: 99 percent / pyridine / CH₂Cl₂ / 3 h / Ambient temperature

3: (S)-BINAPO, Pd₂dba3*CHCl₃ / tetrahydrofuran / 19 h / Ambient temperature

4: 71 percent / sodium naphthalenide / tetrahydrofuran / 0.83 h / -78 °C

5: 45 percent / K₂CO₃ / various solvent(s) / 216 h / 90 °C

With pyridine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; sodium naphthalenide; sodium carbonate; potassium carbonate; (S)-1,1'-binaphthalene-2,2'-diylbis(diphenylphosphine oxide); In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo9701187