{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

Base Information

Chemical Name:{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)
CAS No.:1397711-12-4
Molecular Formula:C₅₇H₄₀N₆O₂Zn
Molecular Weight:906.374
Hs Code.:

Synonyms:{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

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Chemical Property of {2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

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Technology Process of {2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

There total 4 articles about {2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1397711-06-6
{2-[3-ethoxycarbonyl-1-(p-tolyl)-4,5-dihydro-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

: 1397711-12-4
{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 120 ℃; for 15h;
DOI:10.1016/j.tet.2012.07.072

Reference yield:

: 110350-65-7
2-formyl-5,10,15,20-tetraphenylporphyrinato zinc(II)

: 1397711-12-4
{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride

2: potassium carbonate / toluene / 24 h / 120 °C / Inert atmosphere

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 15 h / 120 °C

With sodium hydride; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; 1: Wittig reaction;
DOI:10.1016/j.tet.2012.07.072

Reference yield:

: 58670-19-2
bromo-p-tolylhydrazono-acetic acid ethyl ester

: 1397711-12-4
{2-[3-ethoxycarbonyl-1-(p-tolyl)-1H-pyrazol-5-yl]-5,10,15,20-tetraphenylporphyrinato}zinc(II)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / toluene / 24 h / 120 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 15 h / 120 °C

With potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene;
DOI:10.1016/j.tet.2012.07.072