trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

Base Information

Chemical Name:trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene
CAS No.:861403-98-7
Molecular Formula:C₂₄H₃₀BrNO₄
Molecular Weight:476.411
Hs Code.:

Synonyms:trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

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Technology Process of trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

There total 3 articles about trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 51044-13-4
4-bromobenzyl triphenylphosphonium bromide

: 66749-96-0
4-(1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl)-benzaldehyde

: 861403-98-7
trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1016/j.tetlet.2007.07.127

Reference yield:

: 589-15-1
1-bromomethyl-4-bromobenzene

: 861403-98-7
trans-4-bromo-4'-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-yl)stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: NaH / dimethylformamide

With sodium hydride; In N,N-dimethyl-formamide; 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo035462k