2,2,4,5-tetraphenyl 1,3,2-dioxagermole

Base Information

Chemical Name:2,2,4,5-tetraphenyl 1,3,2-dioxagermole
CAS No.:104284-19-7
Molecular Formula:C₂₆H₂₀GeO₂
Molecular Weight:437.034
Hs Code.:

Synonyms:2,2,4,5-tetraphenyl 1,3,2-dioxagermole

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Chemical Property of 2,2,4,5-tetraphenyl 1,3,2-dioxagermole

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Technology Process of 2,2,4,5-tetraphenyl 1,3,2-dioxagermole

There total 2 articles about 2,2,4,5-tetraphenyl 1,3,2-dioxagermole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: dipotassium cis-1,2-diphenylethylenediolate

: 1613-66-7
dichlorodiphenylgermane

: 104284-19-7
2,2,4,5-tetraphenyl 1,3,2-dioxagermole

Guidance literature:: In diethyl ether; byproducts: KCl; to soln. of K salt in ether added dropwise at 0°C soln. of Ge compd. in dry ether; after stirring for 2,5 h ppt. filtered off; filtrate concd., residue dissolved in benzene and pptd. with hexane;
DOI:10.1002/recl.19881070609

Reference yield: 25.0%

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 39998-10-2
diphenyl bis(diethylamino)germanium

: 104284-19-7
2,2,4,5-tetraphenyl 1,3,2-dioxagermole

Guidance literature:: In tetrahydrofuran; byproducts: (C2H5)2NH; to a soln. of Ge compd. in dry THF was added slowly solid benzoine, after stirring for 1 h at room temp. solvents removed.;
DOI:10.1002/recl.19881070609