propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

Base Information

Chemical Name:propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate
CAS No.:105183-61-7
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:

Synonyms:propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

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Chemical Property of propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

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Technology Process of propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

There total 4 articles about propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-94-5
propyl bromide

: 35677-89-5
benzyl (3S)-2-oxotetrahydro-3-furanylcarbamate

: 105183-61-7
propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1.) water, 23 deg C, 0.5 h, 2.) DMF, 60 deg C, 48 h;
DOI:10.1021/jo00376a001

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 105183-61-7
propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / 1 N aq. NaHCO₃ / 24 h / 23 °C

2: 100 percent / 4-(dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 16 h / 23 °C

3: 1.) NAOH / 1.) water, 23 deg C, 0.5 h, 2.) DMF, 60 deg C, 48 h

With dmap; sodium hydroxide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jo00376a001

Reference yield:

: 35677-88-4
N-benzyloxycarbonyl-(L)-homoserine

: 105183-61-7
propyl L-2-<(carbobenzyloxy)amino>-4-hydroxybutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 4-(dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 16 h / 23 °C

2: 1.) NAOH / 1.) water, 23 deg C, 0.5 h, 2.) DMF, 60 deg C, 48 h

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jo00376a001