(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

Base Information

Chemical Name:(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide
CAS No.:115364-95-9
Molecular Formula:C₂₇H₂₈N₂O₅
Molecular Weight:460.53
Hs Code.:

Synonyms:(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

Chemical Property:

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Technology Process of (S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

There total 4 articles about (S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51871-62-6
(S)-3-tert-butoxycarbonylamino-4-phenylbutanoic acid

: 115364-95-9
(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

2: CH₂Cl₂ / 1 h / 0 °C

3: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

With 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; chloroform;
DOI:10.1021/jm00117a025

Reference yield:

: 60398-41-6
(3S)-tert-butyl 1-benzyl-3-diazo-2-oxopropylcarbamate

: 115364-95-9
(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

Guidance literature:: Multi-step reaction with 4 steps

1: Ag₂O, Na₂CO₃, Na₂S₂O₃*5H₂O / H₂O; dioxane / 1 h / Heating

2: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

3: CH₂Cl₂ / 1 h / 0 °C

4: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

With sodium carbonate; sodium thiosulfate; 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; silver(l) oxide; In 1,4-dioxane; dichloromethane; chloroform; water;
DOI:10.1021/jm00117a025

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 115364-95-9
(S)-N-<2-(benzyloxacarbonyl)-1-oxoethyl>-3-amino-4-phenyl-N'-(benzyloxy)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

2: CH₂Cl₂ / 1 h / 0 °C

3: triethylamine, 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / CHCl₃ / 1.) 0 deg C, 1 h, 2.) room temperature, overnight

With 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; chloroform;
DOI:10.1021/jm00117a025