(S)-<1-2H₁>-2-aminoethanol hydrochloride

Base Information

• Chemical Name: (S)-<1-2H₁>-2-aminoethanol hydrochloride
• CAS No.: 89789-31-1
• Molecular Formula: C₉H₁₃NO
• Molecular Weight: 152.2
• Mol file: 89789-31-1.mol

Synonyms:(S)-<1-2H₁>-2-aminoethanol hydrochloride

Chemical Property of (S)-<1-2H₁>-2-aminoethanol hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (S)-<1-2H₁>-2-aminoethanol hydrochloride

There total 3 articles about (S)-<1-2H₁>-2-aminoethanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(S)-<2-2H1>-O-benzylglycolamide → (S)-<1-2H1>-2-aminoethanol hydrochloride (89789-31-1)

Guidance literature:

With borane; In tetrahydrofuran; for 12h; Heating;

DOI:10.1021/ja00322a037

Reference yield:

benzyl bromide (100-39-0) → (S)-<1-2H1>-2-aminoethanol hydrochloride (89789-31-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 59 percent / Ag₂O / diethyl ether / 42 °C

2: 0.31 g / NH₃ (liq.) / methanol / 144 h / 25 °C

3: 41 percent / BH₃ / tetrahydrofuran / 12 h / Heating

With borane; ammonia; silver(l) oxide; In tetrahydrofuran; methanol; diethyl ether;

DOI:10.1021/ja00322a037

Reference yield:

methyl (S)-<2-2H1>-O-benzylglycolate (89789-27-5) → (S)-<1-2H1>-2-aminoethanol hydrochloride (89789-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.31 g / NH₃ (liq.) / methanol / 144 h / 25 °C

2: 41 percent / BH₃ / tetrahydrofuran / 12 h / Heating

With borane; ammonia; In tetrahydrofuran; methanol;

DOI:10.1021/ja00322a037

upstream raw materials:

benzyl bromide

methyl (S)-<2-2H₁>-O-benzylglycolate